When the wall temperature is very high, a stable vapor film covers the heat transfer surface. The vapor film creates a strong thermal resistance when heat is transferred to the liquid though it. This phenomenon, called "film boiling" is very important in the heat treatment of metals, the design of cryogenic heat exchangers, and the emergency cooling of nuclear reactors. In the practical engineering problems of the transient cooling process of a high temperature wall, the wall temperature history, the variation of the heat transfer coefficients, and the wall superheat at the rewetting points, are the main areas of concern. These three areas are influenced in a complex fashion such factors as the initial wall temperature, the physical properties of both the wall and the coolant, the fluid temperature, and the flow state. Therefore many kinds of specialized experiments are necessary in the creation of precise thermal design. The object of this study is to investigate the heat transfer characteristics in the transient cooling process of a high temperature wall. The slow transient cooling experiment was carried out with a copper block of high thermal capacity. The block was 240 mm high and 79 mm O.D.. The coolant flowed throuogh the center of a 10 mm diameter channel in the copper block. In the copper block, three sheathed thermocouples were placed in a line perpendicular to the flow. These thermocouples were used to take measurements of the temperature histories of the copper block.