Water content of subgrade soil in water supply systems has a large effect on performance. Many researchers lately make use of time-domain reflectometry (TDR) probes to measure the soil water content of subgrade soil from monitoring. The laboratory calibration test of TDR probe should be performed with soil field, because TDR probe can cause an error by type, gradation, density, and temperature of soil. This study shows the laboratory calibration test using TDR CS616, TDR-P3, TDR-T3. The calibration equations of TDR were then proposed. It was confirmed from the study that the data of TDR probe monitored in field could be used to estimate the freezing, unfrozen water content, and matric suction of soil.