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Preparation of photoresist-derived carbon micropatterns by proton ion beam lithography and pyrolysis
Hui-Gyun Nam, Jin-Mook Jung, In-Tae Hwang, Junhwa Shin, Chang-Hee Jung, Jae-Hak Choi 한국탄소학회 Carbon Letters 7 Pages
한국탄소학회 Carbon Letters 2017, Vol.24 8 55-61 (7 pages)
Carbon micropatterns (CMs) were fabricated from a negative-type SU-8 photoresist by proton ion beam lithography and pyrolysis. Well-defined negative-type SU-8 micropatterns were formed by proton ion beam lithography at the optimized fluence of 1×1015 ions cm?2 and then pyrolyzed to form CMs. The crosslinked network structures formed by proton irradiation were converted to pseudo-graphitic structures by pyrolysis. The fabricated CMs showed a good electrical conductivity of 1.58×102 S cm?1 and a... -
Applications of carbon-based materials in solid phase micro-extraction: a review
Jian Guo, Soo-Jin Park, Long-Yue Meng, Xinghua Jin 한국탄소학회 Carbon Letters 8 Pages
한국탄소학회 Carbon Letters 2017, Vol.24 2 10-17 (8 pages)
With continuous development in the field of sample preparation technology, solid phase micro-extraction (SPME) has been widely used in analytical chemistry for high extraction efficiency and convenient operation. Different materials lead to different extraction results. Among existing materials, carbon-based materials are still attracting attention from scientists due to their excellent physical and chemical properties as well as their modifiable surfaces, which could enhance the adsorption... -
Synthesis and characterization of carbon doped TiO₂ photocatalysts supported on stainless steel mesh by sol-gel method
JO. Tijani, OO. Fatoba, TC. Totito, WD. Roos, LF. Petrik 한국탄소학회 Carbon Letters 12 Pages
한국탄소학회 Carbon Letters 2017, Vol.22 6 48-59 (12 pages)
This study synthesized pure anatase carbon doped TiO₂ photocatalysts supported on a stainless steel mesh using a sol-gel solution of 8% polyacrylonitrile (PAN)/dimethylformamide (DMF)/TiCl₄. The influence of the pyrolysis temperature and holding time on the morphological characteristics, particle sizes and surface area of the prepared catalyst was investigated. The prepared catalysts were characterized by several analytical methods: high resolution scanning electron microscopy (HRSEM), energy... -
Effect of carbonization temperature on crystalline structure and properties of isotropic pitch-based carbon fiber
Jung Dam Kim, Jae-Seung Roh, Myung-Soo Kim 한국탄소학회 Carbon Letters 10 Pages
한국탄소학회 Carbon Letters 2017, Vol.21 6 51-60 (10 pages)
Isotropic pitch-based fibers produced from coal tar pitch with the melt-blowing method were carbonized at temperatures ranging from 800 to 1600oC to investigate their crystalline structure and physical properties as a function of the carbonization temperature. The in-plane crystallite size (La) of the carbonized pitch fiber from X-ray diffraction increased monotonously by increasing the carbonization temperature resulting in a gradual increase in the electrical conductivity from 169 to 3800... -
The effect of the spinning conditions on the structure of mesophase pitch-based carbon fibers by Taguchi method
Zhao Jiang, Ting Ouyang, Xiangdong Yao, Youqing Fei 한국탄소학회 Carbon Letters 10 Pages
한국탄소학회 Carbon Letters 2016, Vol.19 11 89-98 (10 pages)
Taguchi’s experimental design was employed in the melt spinning of molten mesophase pitch to produce carbon fibers. The textures of the obtained carbon fibers were radial with varied crack angles, as observed by scanning electron microscopy and polarized optical imaging. The diameter, crack angle, preferred orientation, and tensile modulus of the produced samples were examined to investigate the influence of four spinning variables. The relative importance of the variables has been emphasized... -
Pitch-based carbon fibers from coal tar or petroleum residue under the same processing condition
Jiyoung Kim, Ui-Su Im, Byungrok Lee, Dong-Hyun Peck, Seong-Ho Yoon, Doo-Hwan Jung 한국탄소학회 Carbon Letters 7 Pages
한국탄소학회 Carbon Letters 2016, Vol.19 9 72-78 (7 pages)
successfully prepared from petroleum or coal pyrolysis residues. After pyrolysis fuel oil (PFO), slurry oil, and coal tar were simply filtered to eliminate the solid impurities, the characteristics of the raw materials were evaluated by elemental analysis, 13C nuclear magnetic resonance spectrometer, matrix-assisted laser desorption/ionization time-of-flight mass spectrometer (MALDI-TOF-MS), and so on. Spinnable pitches were prepared for melt-spinning carbon fiber through a simple distillation... -
Effect of fiber-matrix adhesion on the fracture behavior of a carbon fiber reinforced thermoplastic-modified epoxy matrix
H.J. Carrillo-Escalante, A. ?lvarez-Castillo, A. Valadez-Gonz?lez, P. J. Herrera-Franco 한국탄소학회 Carbon Letters 10 Pages
한국탄소학회 Carbon Letters 2016, Vol.19 6 47-56 (10 pages)
known silane, (3-glycidoxy propyl trimethoxysilane) coupling agent. Toughness was determined using the double cantilever test, together with surface analysis after failure using scanning electron microscope. The presence of polysulfone particles improved the fracture behavior of the composite, but fiber-matrix adhesion seemed to play a very important role in the performance of the composite material. There appeared to be a synergy between the matrix modifier and the fibermatrix adhesion coupling... -
Effects of electrochemical oxidation of carbon fibers on interfacial shear strength using a micro-bond method
Dong-Kyu Kim, Kay-Hyeok An, Yun Hyuk Bang, Lee-Ku Kwac, Sang-Yub Oh, Byung-Joo Kim 한국탄소학회 Carbon Letters 8 Pages
한국탄소학회 Carbon Letters 2016, Vol.19 4 32-39 (8 pages)
In this work, we studied the effects of electrochemical oxidation treatments of carbon fibers (CFs) on interfacial adhesion between CF and epoxy resin with various current densities. The surface morphologies and properties of the CFs before and after electrochemical-oxidation-treatment were characterized using field emission scanning electron microscopy, atomic force microscopy, Fourier transform infrared spectroscopy, X-ray photoelectron spectroscopy, and single-fiber contact angle. The... -
Cu²? ion reduction in wastewater over RDF-derived char
Hyung Won Lee, Rae-su Park, Sung Hoon Park, Sang-Chul Jung, Jong-Ki Jeon, Sang Chai Kim, Jin Do Chung, Won Geun Choi, Young-Kwon Park 한국탄소학회 Carbon Letters 7 Pages
한국탄소학회 Carbon Letters 2016, Vol.18 8 49-55 (7 pages)
Refuse-derived fuel (RDF) produced using municipal solid waste was pyrolyzed to produce RDF char. For the first time, the RDF char was used to remove aqueous copper, a representative heavy metal water pollutant. Activation of the RDF char using steam and KOH treatments was performed to change the specific surface area, pore volume, and the metal cation quantity of the char. N2 sorption, Inductively Coupled Plasma-Atomic Emission Spectrometer (ICP-AES), and Fourier transform infrared spectroscopy... -
Sorption behavior of slightly reduced, three-dimensionally macroporous graphene oxides for physical loading of oils and organic solvents
Ho Seok Park, Sung Oong Kang 한국탄소학회 Carbon Letters 6 Pages
한국탄소학회 Carbon Letters 2016, Vol.18 4 24-29 (6 pages)
High pollutant-loading capacities (up to 319 times its own weight) are achieved by three-dimensional (3D) macroporous, slightly reduced graphene oxide (srGO) sorbents, which are prepared through ice-templating and consecutive thermal reduction. The reduction of the srGO is readily controlled by heating time under a mild condition (at 1 10?2 Torr and 200°C). The saturated sorption capacity of the hydrophilic srGO sorbent (thermally reduced for 1 h) could not be improved further even though the...


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