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Effect of carbonization temperature on crystalline structure and properties of isotropic pitch-based carbon fiber
Jung Dam Kim, Jae-Seung Roh, Myung-Soo Kim 한국탄소학회 Carbon Letters 10 Pages
한국탄소학회 Carbon Letters 2017, Vol.21 6 51-60 (10 pages)
function of the carbonization temperature. The in-plane crystallite size (La) of the carbonized pitch fiber from X-ray diffraction increased monotonously by increasing the carbonization temperature resulting in a gradual increase in the electrical conductivity from 169 to 3800 S/cm. However, the variation in the d002 spacing and stacking height of the crystallite (Lc) showed that the structural order perpendicular to the graphene planes got worse in carbonization temperatures from 800 to 1200oC... -
Effect of acid catalysts on carbonization temperatures for ordered mesoporous carbon materials
Jeong Kuk Shon, Xing Jin, Yun Seok Choi, Jong Gu Won, Yoon Kyung Hwang, Dae Jong You, Chengbin Li, Ji Man Kim 한국탄소학회 Carbon Letters 6 Pages
한국탄소학회 Carbon Letters 2016, Vol.20 10 66-71 (6 pages)
polymerize the carbon precursors before the carbonization, an aging process should also be carried out in the presence of acid catalysts in low temperature ranges of 100°C?200°C. In the case of sucrose as a carbon source, sulfuric acid (H2SO4) is typically used as an acid catalyst for the dehydration and subsequent oligomerization of the carbon precursor. This is very important for preventing the infiltrated carbon precursors from draining outside the mesopores of the silica templates before... -
Yield enhancement of matrix precursor in short carbon fiber reinforced randomly oriented carbon/carbon composite
Thakur Sudesh Kumar Raunija, Sharad Chandra Sharma, Anil Verma 한국탄소학회 Carbon Letters 9 Pages
한국탄소학회 Carbon Letters 2016, Vol.19 7 57-65 (9 pages)
system was studied. The fourier transform infrared spectrometry (FTIR), thermogravimetric analysis (TGA), yield, yield rate, and yield impact were used to check the effect of stabilization and pressure on the yield of the matrix precursor and the end properties of the composite thereafter. The results showed that the yield increased with stabilization duration up to 20 h whereas it decreased for stabilization duration beyond 20 h. Further results showed that the stabilized matrix precursor for a... -
Effects of carbonization temperature on pore development in polyacrylonitrile-based activated carbon nanofibers
Hye-Min Lee, Kay-Hyeok An, Byung-Joo Kim 한국탄소학회 Carbon Letters 5 Pages
한국탄소학회 Carbon Letters 2014, Vol.15 No.2 13 146-150 (5 pages)
In this work, activated carbon nanofiber (ACNF) electrodes with high double-layer capacitance and good rate capability were prepared from polyacrylonitrile nanofibers by optimizing the carbonization temperature prior to H2O activation. The morphology of the ACNFs was observed by scanning electron microscopy. The elemental composition was determined by analysis of X-ray photoelectron spectroscopy. N2-adsorption-isotherm characteristics at 77 K were confirmed by Brunauer-Emmett-Teller and... -
열중량분석법을 이용한 하수슬러지 탄화물의 연소특성 평가
박소미, 임혁, 김철규 한국열환경공학회 한국열환경공학회 학술대회지 10 Pages
한국열환경공학회 한국열환경공학회 학술대회지 2015년 추계 3 16-25 (10 pages)
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석탄과 EFB 반탄화물의 혼합 연소에 따른 발생가스 특성
최병수, 구재회, 임용택, 오세천 한국열환경공학회 열환경공학 9 Pages
한국열환경공학회 열환경공학 2016, 제 13권 1호 8 53-61 (9 pages)
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열중량분석법을 이용한 하수슬러지 탄화물의 연소 특성 평가
박소미, 임혁, 김철규 한국열환경공학회 열환경공학 9 Pages
한국열환경공학회 열환경공학 2015, 제 12권 2호 9 74-82 (9 pages)
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볏짚 이용 Bio-SRF 활용을 위한 Torrefaction 반응 특성 연구
남성방, 임용택, 구재회, 남상익, 김윤명, 오세천, Jeeban Poudel 한국열환경공학회 열환경공학 8 Pages
한국열환경공학회 열환경공학 2015, 제 12권 2호 4 25-32 (8 pages)
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종이가 주성분인 RDF(Refuse Derived Fuel)의 탄화특성
최연석, 김부웅 한국열환경공학회 열환경공학 6 Pages
한국열환경공학회 열환경공학 2005, 제 2권 2호 4 107-112 (6 pages)
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바이오메스 열처리 및 수열합성에 의한 복합기공소재 제조
서정권, 이정민 한국열환경공학회 열환경공학 16 Pages
한국열환경공학회 열환경공학 2006, 제 3권 1호 5 39-54 (16 pages)
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Pitch 열개질에 의한 탄소계 전극소재 합성
서정권, 홍지숙, 이정민, 이범재 한국열환경공학회 열환경공학 15 Pages
한국열환경공학회 열환경공학 2006, 제 3권 2호 1 93-108 (15 pages)
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Pitch 열개질에 의한 탄소계 전극소재 합성
서정권, 홍지숙, 이정민, 이범재 한국열환경공학회 열환경공학 15 Pages
한국열환경공학회 열환경공학 2009, 제 6권 1호 5 41-55 (15 pages)
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Graphitization of PAN-based carbon fibers by CO₂ laser irradiation
Liangbo Yao, Weimin Yang, Sanyang Li, Yang Sha, Jing Tan, Ying An, Haoyi Li 한국탄소학회 Carbon Letters 6 Pages
한국탄소학회 Carbon Letters 2017, Vol.24 13 97-102 (6 pages)
high specific modulus that have attracted much interest in the aerospace industry, but their high manufacturing cost and low yield are still problems that prevent their wide applications in practice. This paper presents a laser-based process for graphitization of carbon fiber (CF) and explores the effect of laser radiation on the microstructure of CF. The obtained Raman spectra indicate that the outer surface of CF evolves from turbostratic structures into a three-dimensional ordered state after... -
Physicochemical properties and methane adsorption performance of activated carbon nanofibers with different types of metal oxides
Faten Ermala Che Othman, Norhaniza Yusof, Hasrinah Hasbullah, Juhana Jaafar, Ahmad Fauzi Ismail, Noor Shawal Nasri 한국탄소학회 Carbon Letters 8 Pages
한국탄소학회 Carbon Letters 2017, Vol.24 11 82-89 (8 pages)
In this study, composite PAN-based ACNFs embedded with MgO and MnO2 were prepared by the electrospinning method. The resultant pristine ACNFs, ACNF/MgO and ACNF/MnO2 were characterized in terms of their morphological changes, SSA, crystallinity and functional group with FESEM-EDX, the BET method, XRD and FTIR analysis, respectively. Results from this study showed that the SSA of the ACNF/MgO composite (1893 m2 g?1) is significantly higher than that of the pristine ACNFs and ACNF/MnO2 which is... -
Relationships between dielectric properties and characteristics of impregnated and activated samples of potassium carbonate- and sodium hydroxide-modified palm kernel shell for microwave-assisted activation
Norulaina Alias, Muhammad Abbas Ahmad Zaini, Mohd Johari Kamaruddin 한국탄소학회 Carbon Letters 11 Pages
한국탄소학회 Carbon Letters 2017, Vol.24 9 62-72 (11 pages)
The aim of this work was to evaluate the dielectric properties of impregnated and activated palm kernel shells (PKSs) samples using two activating agents, potassium carbonate (K2CO3) and sodium hydroxide (NaOH), at three impregnation ratios. The materials were characterized by moisture content, carbon content, ash content, thermal profile and functional groups. The dielectric properties were examined using an open-ended coaxial probe method at various microwave frequencies (1?6 GHz) and... -
Preparation of photoresist-derived carbon micropatterns by proton ion beam lithography and pyrolysis
Hui-Gyun Nam, Jin-Mook Jung, In-Tae Hwang, Junhwa Shin, Chang-Hee Jung, Jae-Hak Choi 한국탄소학회 Carbon Letters 7 Pages
한국탄소학회 Carbon Letters 2017, Vol.24 8 55-61 (7 pages)
Carbon micropatterns (CMs) were fabricated from a negative-type SU-8 photoresist by proton ion beam lithography and pyrolysis. Well-defined negative-type SU-8 micropatterns were formed by proton ion beam lithography at the optimized fluence of 1×1015 ions cm?2 and then pyrolyzed to form CMs. The crosslinked network structures formed by proton irradiation were converted to pseudo-graphitic structures by pyrolysis. The fabricated CMs showed a good electrical conductivity of 1.58×102 S cm?1 and a... -
Catalytic hydrogenation-assisted preparation of melt spinnable pitches from petroleum residue for making mesophase pitch based carbon fibers
Dong Hun Lee, Jisu Choi, Young Se Oh, Yoong Ahm Kim, Kap Seung Yang, Ho Jin Ryu, Yong Jung Kim 한국탄소학회 Carbon Letters 8 Pages
한국탄소학회 Carbon Letters 2017, Vol.24 4 28-35 (8 pages)
We demonstrated an effective way of preparing melt spinnable mesophase pitches via catalytic hydrogenation of petroleum residue (fluidized catalytic cracking-decant oil) and their subsequent thermal soaking. The mesophase pitches thus obtained were analyzed in terms of their viscosity, elemental composition, solubility, molecular weight, softening point and optical texture. We found that zeolite-induced catalytic hydrogenation under high hydrogen pressure contributed to a large variation in the... -
Preparation of carbon discs using petroleum-based binder pitch reformed with carbon black
Sangmin Lee, Kyung Hoon Kim, Young-Seak Lee 한국탄소학회 Carbon Letters 4 Pages
한국탄소학회 Carbon Letters 2017, Vol.23 13 84-87 (4 pages)
Carbon materials are widely used in various industry applications, such as a carbon fibers, graphite brushes, aluminum engineering and binders, because carbon materials have high specific strength, high conductivity, excellent thermal shock resistance, and other favorable properties [1-4]. These carbon materials are prepared from various precursors, such as polyacrylonitrile (PAN), phenolic resins and pitches. Among these precursors, pitches are more economical than PAN and phenol resin, and it... -
Facile fabrication of electrospun polyacrylonitrile/ poly(vinylidene fluoride)-based carbon nanofibers for supercapacitor electrodes
Hyo In Lee, Soo-Jin Park 한국탄소학회 Carbon Letters 5 Pages
한국탄소학회 Carbon Letters 2017, Vol.23 12 79-83 (5 pages)
Energy storage devices and renewable energy sources are some of the most interesting alternatives being developed to solve the energy crisis [1,2]. At the same time, energy harvesting and storage devices are among the technologies with the highest potential to efficiently satisfy the energy requirements of compact electronic devices [3]. Among various energy storage devices, supercapacitors are the among the most intensely researched because of their high power density, long cycle retention, and... -
Lyocell-based activated carbon fibers improved the adsorption of harmful gas properties when produced via dual-simultaneous treatments
Byong Chol Bai, Ji Sun Im, Young-Seak Lee 한국탄소학회 Carbon Letters 5 Pages
한국탄소학회 Carbon Letters 2017, Vol.23 10 69-73 (5 pages)
In gas adsorption processes, activated carbon fibers (ACFs) are used for the adsorption of the harmful gases that are generated by coal or oil combustion, and they have been widely studied [1,2]. ACFs have been used for harmful gas removal because of their specific surface area, micropores, reproducibility, safety, and processing ability, which are beneficial properties for a wide range of applications [3,4]. -
Effect of added mesophase pitch during the pitch synthesis reaction of PFO
Ji Hong Kim, Jong Gu Kim, Chul Wee Lee, Ki Bong Lee, Ji Sun Im 한국탄소학회 Carbon Letters 7 Pages
한국탄소학회 Carbon Letters 2017, Vol.23 7 48-54 (7 pages)
This research considers the effect of added mesophase pitch (MP) as an additive during the pitch synthesis reaction of pyrolyzed fuel oil (PFO). Two effects are generated by adding MP. One is an enhancement of thermal stability due to the high thermal property of the additive; the other is that the volatile compounds that were removed by vaporization of PFO during the thermal reaction can participate in the pitch synthesis reaction (PFO→pitch) more efficiently. The effect differs according to... -
Extraction and characterization of lignin from black liquor and preparation of biomass-based activated carbon therefrom
Daeyeon Kim, Jinsil Cheon, Jeonghoon Kim, Daekyun Hwang, Ikpyo Hong, Oh Hyeong Kwon, Won Ho Park, Donghwan Cho 한국탄소학회 Carbon Letters 8 Pages
한국탄소학회 Carbon Letters 2017, Vol.22 14 81-88 (8 pages)
possible fusion between the lignin particles occurring upon carbonization. The carbonized and then pulverized lignin exhibits brittle surfaces, the increased thermal stability, and the carbon assay with increasing the carbonization temperature. The scanning electron microscopic images and the Brunauer-Emmett-Teller result indicate that the steam-activated carbon has the specific surface area of 1718 m2/g, which is markedly greater than the carbonized lignin. This study reveals that biomassbased... -
Adsorption characteristics of heavy metals ions by physical activation on coal tar pitch-based activated carbon fibers
Bo-kyung Choi, Jae-Kyoung Ko, Soo-Jin Park, Min-Kang Seo 한국탄소학회 Carbon Letters 5 Pages
한국탄소학회 Carbon Letters 2017, Vol.22 10 96-100 (5 pages)
Due to the increasing population growth of modern society, along with rapid industrial development and urbanization, environmental pollution continues to worsen and has become an important issue, not only domestically but also worldwide. In particular, toxic substances such as heavy metal ions are present in the wastewater produced by various industries. This wastewater flows into rivers, pollutes water supplies, and can contaminate the drinking water supplied to people [1-3]. Powder or... -
High-energy-density activated carbon electrode for organic electric-double-layer-capacitor using carbonized petroleum pitch
Poo Reum Choi, Sang-Gil Kim, Ji Chul Jung, Myung-Soo Kim 한국탄소학회 Carbon Letters 11 Pages
한국탄소학회 Carbon Letters 2017, Vol.22 8 70-80 (11 pages)
at a medium carbonization temperature. Therefore, it was possible to control the crystalline structure, SSA, and pore structure of AC by changing the pre-carbonization temperature. Because the electrode density increased with increasing of the pre-carbonization temperature, the highest volumetric capacitance of 28.4 F/cc was obtained from the PP pre-carbonized at 700°C, exhibiting a value over 150% of that of a commercial AC (MSP-20) for EDLC. Electrochemical activation was observed from the... -
Nitrogen-doped carbon nanosheets from polyurethane foams and removal of Cr(VI)
Jiaqi Duan, Baohua Zhang, Huailin Fan, Wenzhong Shen, Shijie Qu 한국탄소학회 Carbon Letters 10 Pages
한국탄소학회 Carbon Letters 2017, Vol.22 7 60-69 (10 pages)
hydrothermal carbonization following ZnCl2 chemical activation. Scanning electron microscopy, thermogravimetric analysis, Fourier transform infrared spectroscopy, solid state 13C nuclear magnetic resonance (NMR) spectra and X-ray photoelectron spectroscopy were used to characterize the nitrogen-doped carbon nanosheet structure and composition. The removal of Cr(VI) by the N-doped carbon nanosheets was investigated. The results showed that the maximum removal capacity for chromium of 188 mg/g was... -
Synthesis and characterization of carbon doped TiO₂ photocatalysts supported on stainless steel mesh by sol-gel method
JO. Tijani, OO. Fatoba, TC. Totito, WD. Roos, LF. Petrik 한국탄소학회 Carbon Letters 12 Pages
한국탄소학회 Carbon Letters 2017, Vol.22 6 48-59 (12 pages)
This study synthesized pure anatase carbon doped TiO₂ photocatalysts supported on a stainless steel mesh using a sol-gel solution of 8% polyacrylonitrile (PAN)/dimethylformamide (DMF)/TiCl₄. The influence of the pyrolysis temperature and holding time on the morphological characteristics, particle sizes and surface area of the prepared catalyst was investigated. The prepared catalysts were characterized by several analytical methods: high resolution scanning electron microscopy (HRSEM), energy... -
Thermo-electrical properties of randomly oriented carbon/carbon composite
Thakur Sudesh Kumar Raunija, N. Supriya 한국탄소학회 Carbon Letters 11 Pages
한국탄소학회 Carbon Letters 2017, Vol.22 3 25-35 (11 pages)
properties of low cost and rapidly produced randomly oriented carbon/carbon (C/C) composite. The composite body was fabricated by combining the high-pressure hot-pressing (HP) method with the lowpressure impregnation thermosetting carbonization (ITC) method. After the ITC method step selected samples were graphitized at 3000°C. Detailed characterization of the samples’ physical properties and thermal properties, including thermal diffusivity, thermal conductivity, specific heat and coefficient... -
The effects of carbon coating onto graphite filler on the structure and properties of carbon foams
Ji-Hyun Kim, Do Young Kim, Young-Seak Lee 한국탄소학회 Carbon Letters 5 Pages
한국탄소학회 Carbon Letters 2017, Vol.21 16 111-115 (5 pages)
Carbon foams (CFms) are of crucial importance in electrical and mechanical devices due to their high thermal conductivity used for eliminating high heat flow and maintaining low temperatures [1]. The most common CFms are types of aluminum alloys, copper and diamond. However, the mechanical properties of metal-based heat sink materials are difficult to control at temperatures over 550°C [2,3]. Thus, CFms are actively investigated as heat sink materials because of their good properties, such as... -
Green synthesis of fluorescent carbon dots from carrot juice for in vitro cellular imaging
Yang Liu, Yanan Liu, Mira Park, Soo-Jin Park, Yifan Zhang, Md Rashedunnabi Akanda, Byung-Yong Park, Hak Yong Kim 한국탄소학회 Carbon Letters 7 Pages
한국탄소학회 Carbon Letters 2017, Vol.21 7 61-67 (7 pages)
surfaces of obtained CDs were highly covered with hydroxyl groups and nitrogen groups without further modification. The quantum yield of as-obtained CDs was as high as 5.16%. The cell viability of HaCaT cells against a purified CD aqueous solution was higher than 85% even at higher concentration (700 μg mL?1) after 24 h incubation. Finally, CD cultured cells exhibited distinguished blue, green, and red colors, respectively, during in vitro imaging when excited by three wavelength lasers under a... -
Morphologies and surface properties of cellulose-based activated carbon nanoplates
Seulbee Lee, Min Eui Lee, Min Yeong Song, Se Youn Cho, Young Soo Yun, Hyoung-Joon Jin 한국탄소학회 Carbon Letters 7 Pages
한국탄소학회 Carbon Letters 2016, Vol.20 5 32-38 (7 pages)
CNPs showed a relatively high char yield when compared with MCC due to sulfate functional groups introduced during the manufacturing process. In addition, pyrolyzed CNPs (CCNPs) showed more effective chemical activation behavior compared with MCC-induced carbonaceous materials. The activated CCNPs exhibited a microporous carbon structure with a high surface area of 1310.6 m2/g and numerous oxygen heteroatoms. The results of this study show the effects of morphology and the surface properties of... -
Pitch-based carbon fibers from coal tar or petroleum residue under the same processing condition
Jiyoung Kim, Ui-Su Im, Byungrok Lee, Dong-Hyun Peck, Seong-Ho Yoon, Doo-Hwan Jung 한국탄소학회 Carbon Letters 7 Pages
한국탄소학회 Carbon Letters 2016, Vol.19 9 72-78 (7 pages)
a simple distillation under strong nitrogen flow, and further vacuum distillation to obtain a high softening point. Carbon fibers were produced from the above pitches by single-hole melt spinning and additional heat treatment, for oxidization and carbonization. Even though spinnable pitches and carbon fibers were processed under the same conditions, the melt-spinning and properties of the carbon fiber were different depending on the raw materials. A fine carbon fiber could not be prepared from... -
Cellulose-based carbon fibers prepared using electron-beam stabilization
Min Il Kim, Mi-Seon Park, Young-Seak Lee 한국탄소학회 Carbon Letters 6 Pages
한국탄소학회 Carbon Letters 2016, Vol.18 9 56-61 (6 pages)
measured. The structure of the cellulose fibers was determined to have changed to hemicellulose and cross-linked cellulose as a result of the E-beam stabilization. The hemicellulose decreased the initial decomposition temperature, and the cross-linked bonds increased the carbonization yield of the cellulose fibers. Increasing the absorbed E-beam dose to 1500 kGy increased the carbonization yield of the cellulose-based carbon fiber by 27.5% upon exposure compared to untreated cellulose fibers. -
Microwave-assisted pretreatment technologies for the conversion of lignocellulosic biomass to sugars and ethanol: a review
Pradeep Puligundla, Sang-Eun Oh, Chulkyoon Mok 한국탄소학회 Carbon Letters 10 Pages
한국탄소학회 Carbon Letters 2016, Vol.17 No.1 1 1-10 (10 pages)
Lignocellulosic biomass conversion to biofuels such as ethanol and other value-added bio-products including activated carbons has attracted much attention. The development of an efficient, cost-effective, and eco-friendly pretreatment process is a major challenge in lignocellulosic biomass to biofuel conversion. Although several modern pretreatment technologies have been introduced, few promising technologies have been reported. Microwave irradiation or microwave-assisted methods (physical and...
