To shield the radiation, we can make use of various materials, but the scattered rays can be caused by the shielding materials. The degree of the scattered rays production is influenced by the nature of the shielding materials and the energy of the radiation, therefore to choose the proper shielding material is the most important matter in radiation protection. Authors made an experimental study on the scattered rays generated from the shielding materials, and obtained the results as follows: 1. In the ranking of the scattered rays production: Cement bricks, black colored fire bricks, and red colored fire bricks were marked the first the second, and the third ranking respectly, and the last order was lead plates. 2. In the relative ranking of the scattered rays production by energy increase: Lead plates were marked the first order, the next and third order were red colored fire bricks and black colored fire bricks respectly, and cement bricks were marked the last order. 3. The scattered ray ratio of lateral-back point per lateral point were generally decreased by energy increment. The diminishing orders were that lead plates were the first order, and the next and the third order were red colored fire bricks and black colored fire bricks respectly, cement bricks were marked the last order.