- 한국산 천연원료로부터 $eta$-Sialon의 합성 및 그 특성
- ㆍ 저자명
- 임헌진,이홍림
- ㆍ 간행물명
- 요업학회지
- ㆍ 권/호정보
- 1989년|26권 3호|pp.402-408 (7 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
$eta$-Sialon powder was synthesized by the simultaneous reduction and nitridation of the mixed powder of Hadong kaolin and Kimcheon quartzite, using graphite as a reducing agent. The synthesized $eta$-Sialon powder (Z=1) was hot-pressed at 175$0^{circ}C$, for 90min under 30MPa in N2 atmosphere, after Yttria and YAG composition material were added as sintering agents. The effects of grain-boundary crystallization on high-temperature mechanical properties of $eta$-Sialon ceramics were investigated. Strength degradation was observed at above 1,00$0^{circ}C$ for the $eta$-Sialon (Z=1)-8wt% Y2O3 composition, but it was not observed up to 1,20$0^{circ}C$ for the $eta$-Sialon-8wt% YAG composition which was annealed at 1,40$0^{circ}C$ for 4 hours in N2 atmosphere. After the $eta$-Sialon-8wt% YAG composition was annealed, the decrease of fracture toughness was observed.