- 분무열분해법에 의한 MgO 첨가 $Al_2O_3$ 분체합성 및 소결성에 관한 연구
- ㆍ 저자명
- 박정현,조경식,송규호
- ㆍ 간행물명
- 요업학회지
- ㆍ 권/호정보
- 1990년|27권 4호|pp.501-512 (12 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
Al2O3 and 0.25wt% MgO-doped Al2O3 powders were made from the alcohol solution of Al(NO3)3.9H2O and Mg(NO3)2.6H2O by spray pyrolysis method. Each powder was prepared at 900 and 100$0^{circ}C$. Powders prepared at 90$0^{circ}C$ were amorphous phase, but prepared at 100$0^{circ}C$ wre mainly ${gamma}$-Al2O3 crystalline form. Particle size of the MgO-doped Al2O3 powders was in the range of 0.2-2${mu}{ extrm}{m}$, but undooped powders shwoed comparatively wider range of particle size. All the powders prepared at 900 and 100$0^{circ}C$ were transformed to $alpha$-Al2O3 crystalline form by calcination at 110$0^{circ}C$ for 1hr. Each powder was sintered at 1600, 1650 and 1$700^{circ}C$ for 2hrs. MgO-doped Al2O3 body sintering at 1$650^{circ}C$ showed 99% of relative density but undooped Al2O3 showed 95% of relative density, even sintered at higher temperature of 1$700^{circ}C$.