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공침법에 의한 Cordierite분말의 합성 및 소결에 관한 연구
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  • 공침법에 의한 Cordierite분말의 합성 및 소결에 관한 연구
저자명
한문희,박금철
간행물명
요업학회지
권/호정보
1990년|27권 7호|pp.899-906 (8 pages)
발행정보
한국세라믹학회
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

The cordierite powders were prepared from Mg(NO3)2.6H2O, Al(NO3)3.9H2O and colloidal silica by the coprecippitation method, and the sintering behavior of the powders were investigated. Two different methods were applied for producing the precursor powders. The one was to added the aqueous solution of Mg(NO3)2.6H2O and Al(NO3)3.9H2O to NH4OH to adjust pH at 10 where the colloidal silica of pH 10 was added. The other wa to add the aqueous solution of Mg(NO3)2.6H2O and Al(NO3)3.9H2O to the colloidal silica with NH4OH to control the final mixture to be at pH 10. It was confirmed that more homogeneous powders were obtained from the latter method. The firing linear shrinkage of the powder compacts fabricated from the calcined powder between 90$0^{circ}C$ and 110$0^{circ}C$ was found to be larger as the calcination temperature was low. But all of them stopped shrinking around 120$0^{circ}C$. The powder compacts, fabricated using the calcined powders at 90$0^{circ}C$ and 95$0^{circ}C$ for 2hours and sintered at 142$0^{circ}C$ for 2hours, showed relative density of 93-96%, 3-point bending strength of 81-83MPa, KIC of 1.9-2.4 MPam1/2 and thermal expansion coefficient of 0.213-0.732$ imes$10-6$^{circ}C$.