- 완도납석과 알콕사이드로부터 제조된 $eta$-Sialon 세라믹스의 기계적 성질
- ㆍ 저자명
- 이홍림,손연하,임헌진
- ㆍ 간행물명
- 요업학회지
- ㆍ 권/호정보
- 1991년|28권 5호|pp.390-398 (9 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
$eta$-Sialon powder was prepared from Wando pyrophyllite by the carbothermic reduction and nitridation at 135$0^{circ}C$ for 10 h nitrogen atmosphere. Amorphous silica prepared from Si(OC2H5)4 was added to Wando pyrophyllite powder in order to control the final Z value. Two different methods were applied for synthesis of $eta$-sialon powders. In Process A, the amorphous silica prepared from Si(OC2H5)4 was admixed to Wando pyrophyllite powder. Process B was started from the mixture of Wando Y2O3 was added to the synthesized $eta$-Sialon powders as a sintering aid, and the mixed powders were hot pressed at 175$0^{circ}C$ for 120 min in nitrogen atmosphere under 30 MPa. Their mechanical properties were compared. The maximum values of M.O.R., hardness and KIC were 667 MPa, 16 GPa and 6.3 MN/m3/2, respectively, and they are the values obtained form $eta$-Sialon ceramics prepared by process A of Z=0.5.