- 플라즈마 화학증착에 의한 강재위에 TiN의 저온증착
- ㆍ 저자명
- 이정래,김광호,조성재
- ㆍ 간행물명
- 요업학회지
- ㆍ 권/호정보
- 1993년|30권 2호|pp.148-156 (9 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
TiN films were deposited onto high speed steel (SKH9) by plasma assisted chemical vapor deposition (PACVD) using a TiCl4/N2/H2/Ar gas mixture at around 50$0^{circ}C$. The effects of the deposition temperature, R.F. power and TiCl4 concentration on the deposition of TiN and the microhardness of TiN film were investigated. The crystallinity and the microhardness of TiN films were improved with increase of the deposition temperature. Optimum deposition temperature in this study was 50$0^{circ}C$, because a softening or phase transformation of the substrate occurred over 50$0^{circ}C$. A large increase of the film growth rate with a strong(200) preferred orientation was obtained by increasing R.F. power. Much chlorine content of about 10at.% was found in the deposited films and resulted in relatively low average microhardness of about 1, 500Kgf/$ extrm{mm}^2$ compared with the theoretical value(~2, 000Kgf/$ extrm{mm}^2$).