This study was performed at Sa-Sang Industrial area in Pusan City. To measure the total suspended particulates(T.S.P) and $SO_3$ following places was selected industrial area, down town, residentail area. T.S.P was collected on glass filters by High-Volume Air Sampler, $SO_3$ was measured by PbO2 Candle method. The collected T.S.P was analyzed for various anlon(for example, $NO_3$, $SO_4$, $PO_4$, F, Cl) by ion Chromatography, and Pb by Inductively Coupled Plasma.