- 소결시의 승온속도가 질화규소 요업체의 미세조직과 파괴인성에 미치는 영향
- ㆍ 저자명
- 이상훈,이재도,김도연
- ㆍ 간행물명
- 요업학회지
- ㆍ 권/호정보
- 1995년|32권 11호|pp.1227-1232 (6 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
Effect of heating rate on the microstructure of the silicon nitride ceramics has been investigated. The specimens with composition of 92Si3N4-6Y2O3-2Al2O3 (in wt%) were sintered at 176$0^{circ}C$ under 127 kPa for 3h in N2 atmosphere at various heating rates from 1 to 10$0^{circ}C$/min. The grain size of larger than 2${mu}{ extrm}{m}$ and less than 1${mu}{ extrm}{m}$ were measured and compared for the specimens. Regardless of heating rate, grain size of all the specimens showed bimodal distributions and the fracture toughness remained in the range of 5.53~5.72 MPa.m1/2. However, the aspect ratio of the grains of diameter above 2${mu}{ extrm}{m}$ increased with the heating rate while their grain size and volume fraction decreased.