- 철계 액상을 통한 붕화지르코늄의 소결
- ㆍ 저자명
- 우상국,한인섭,김흥수,양준환,강을손,김종희
- ㆍ 간행물명
- 요업학회지
- ㆍ 권/호정보
- 1996년|33권 3호|pp.259-268 (10 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
In the present study the effect of the addition of Fe on the pressureless and hot press sintering behavior was studied under Ar atmosphere. Pressureless sintering was performed 1900~220$0^{circ}C$ under. Ar atmosphere. The addition of 1 wt% Fe was increased effectively of the sintered density. However it was impossible to obtain high density higher than 90%,. Zr-Fe-B compound in liquid phase was observed from the EDS and WDS analysis. It was considered that sinterability was enhanced due to the mass transfer through Fe based liquid phase formed at the sintering temperature. Hot pressing was performed at 1600~1$700^{circ}C$ under Ar atmos-phere for 1 hr. It was possible obtain 95% relative density of ZrB2 specimen which is higher density at pressure-less sintering. It could be thought that ZrB2 particles was rearranged through liquid phase by applied pressure during initial stage of sintering.