- 졸-겔법에 의한 $gamma-LiAlO_2$ 단섬유의 제조
- ㆍ 저자명
- 현상훈,이재현,홍성안
- ㆍ 간행물명
- 요업학회지
- ㆍ 권/호정보
- 1996년|33권 10호|pp.1079-1088 (10 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
Discontinuous ${gamma}$-LiAlO2 fibers for fiber-reinforcing MCFC matrixes have been produced by the sol-gel process using the centrifugal spinning apparatus of the Rotary type. Gel fibers could be obtained through spinning of stable LiAlO2 complex polymetric sols under the optimum spinning conditions (hollow-disc rotating velocity 9000 rpm sol feeding rate of 4ml/min flowing N2 temperature of 4$0^{circ}C$ and flowing N2 pressure of 4 bar). It was found that defect free and densified ${gamma}$-LiAlO2 fibers with the relative density of 98% and the mean diameter of 4.7${mu}{ extrm}{m}$ were prepared when the spinned fibers were heat-treated to 100$0^{circ}C$ on the specified heating schedule. in particular the mean diameter and length of fibers could be controlled by the pressure of flowing N2 and the chopping-sieving method respectively.