Recently carbon fiber reinforced plastic (CFRP) has been used structural materials in corrosive environment such as for water, chemical tank and pipes. However, mechanical properties of such materials may be change when CFRP and exposed to corrosive environment for long periods of time. The degradation behavior of carbon fiber/epoxy resin composite material in distilled water is investigated using acoustic emission (AE) technique, Fracture toughness tests are performed on the compact tension specimens that are pilled by two types of $[O_2/9O_2]_{3s}$ and $[O/9O]_6s$. During the testes, AE test was carried out to monitor the damage of CFRP by moisture absorption. The data was treated by 2-parameter Weibull distribution and the fracture surface was observed by scanning electron microscope.