This study was conducted for an efficient utilization of waste fly ash obtained from the power plant. Fly ash was used for synthesizing zeolite. Na-P1 zeolite could be easily synthesized from waste fly ash and showed the potential to remove heavy metal ions. The synthetic zeolite showed good adsorption property for heavy metal much better than raw fly ash and natural zeolites. Na-P1 exhibited the high adsorption efficiency with a maximum value of 260 Pb mg/g and strong affinity for $Pb^{2+}$ ion. The metal ion selectivity of Na-P1 was determined in a decreasing order : $Pb^{2+}>Cd^{2+}>Cu^{2+}>Zn^{2+}>Fe^{3+}.$