An experimental study has been carried out to obtain optimal conditions for turbulent mixing of two fluid streams at various angle branches by a flow visualization method. The main purpose of this study is the utilization of flow visualization method as a fast and efficient way to find the optimal mixing conditions when several flow control parameters are superimposed. It is verified that the optimal conditions estimated by flow visualization method have good agreement with the concentration field measurements. The results demonstrate that the diameter ratio is mainly attributed to the mixing phenomena than the branch pipe angle and the Reynolds number. The most striking fact is that there exists the best diameter ratio, d/D.ident. O.17, which requires the minimum momentum ratio in the range of the present experiment. The velocity ratio for the optimal mixing condition has a value within 2 to 16 according to the different flow parameters.