- 질화규소의 기계적 성질 및 접촉 손상: I. ${alpha}/{eta}$ 상분율의 영향
- ㆍ 저자명
- 이승건
- ㆍ 간행물명
- 한국분말야금학회지
- ㆍ 권/호정보
- 1998년|5권 1호|pp.15-21 (7 pages)
- ㆍ 발행정보
- 한국분말야금학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
The effect of $alpha$/$eta$ phase on the mechanical properties and contact damage of silicon nitrides $Si_3N_4$) was investigated. Silicon nitride materials were prepared from two starting powders, at selective increasing hot-pressing temperatures to coarsen the microstructures: (i) from relatively coarse $alpha$-phase powder, essentially equiaxed $alpha$-$Si_3N_4$ grains, with limited, slow transformation to $eta$-$Si_3N_4$ grain; (ii) from relatively fine $alpha$-phase powder, a more rapid transformation to $eta$-$Si_3N_4$, with attendant grain elongation. The resulting micro-structure thereby provided a spectrum of $alpha$/$eta$ phase ratios, grain sizes, and grain shapes. Fracture strength, hardness, and toughness were measured, and contact damage and strength degradation after indentation were investigated by Hertzian indentation using spherical indenter. A brittle to ductile transition in $Si_3N_4$ depended on $alpha$/$eta$ phase ratio as well as grain size. Silicon nitride with elongated $eta$ grains showed a superior, contact damage resistance.