The knock in a spark ignition engine has been investigated to avoid the damage to the engine and unpleasant feeling caused by the pressure waves propagating across the combustion chamber. Knock intensity and knock onset angle were used as physical parameters to quantify the knock characteristics. The knock intensity is defined as a peak to peak value of the bank pass filtered combustion pressure signal and the knock onset angle is determined as the crank angle at which this signal exceeded the threshold level on each cycle. The cyclic variation of knock in four valve single cylinder engine was investigated with these two parameters. The location of autoignition was also examined by ion probes in the cylinder head gasket and squish region in the combustion chamber. For this measurement, a single cylinder engine was modified to accept the pressure transducer, 18 ion probes in the squish region and 8 ion probes in the specially designed PCB (Printed ulcornerCircuit Board) cylinder head gasket.