Comparative effects of gamma irradiation and methyl bromide (MBr) fumigation on disinfestation and some physicochemical attributes of acorn seeds were investigated. Insects in domestic acorns were identified to be Curculio dentipes Roelofs and Dichocrocis punctiferalis Guenee, which were easily disinfestated immediately after commercial MBr fumigation. Irradiation also showed similar effects on mortality of the insects in different post-irradiation periods; at 3rd day with doses of 1-3 kGy and at around 30th day 0.5-1 kGy. MBr fumigation caused the decrease in lightness (Hunter L value), total phenolics and reducing sugars and the increase in yellowness (Hunter b value) and browning intensity for the subjected samples, as compared with the nontreated control and irradiated ones at 0.5-2 kGy. Furthermore, MBr fumigation resulted in decay for the most part of samples during storage at 5-10 $^{circ}C$ for 6 months in a PVC box packaging with nets. As a result, optimum levels of irradiation is expected to be roe of the alternatives to chemical fumigants.