Correlations of drop size and velocity in a spray from the disintegration of liquid jet and liquid film from an internal mixing twin-fluid atomizer, were determined by phase Doppler method. The distribution pattern of Sauter mean diameter(SMD) in a spray was changed by a behavior of liquid flow. As smaller droplets became faster and slower easily by the surrounding conditions, the correlation between drop size and mean velocity was found to be varied as next 3 steps; firstly smaller droplets have a higher mean velocity at the area near atomizer, droplets have almost the same mean velocity and finally larger droplets have a higher mean velocity at the area far from an atomizer.