The determination method of successful operation conditions to control the temperature and pressure in autoclave after non-taping vulcanization process was represented. Heat and mass balances were constructed to predict the mass flow rates of air, steam, and condensed water into or from autoclave when the temperature and pressure in the autoclave were to be controlled in the desired profiles. The balance equations were solved by appropriate mathematics, and the solution was applied to an autoclave system where the temperature and pressure were linearly decreased. The resulting solutions were illustrated in graphs.