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GC/MS와 GC/ECD를 이용한 한약재 중 잔류 농약의 분석
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  • GC/MS와 GC/ECD를 이용한 한약재 중 잔류 농약의 분석
저자명
김호경,박소연,고병섭,Kim. Ho-Kyoung,Park. So-Yeon,Ko. Byoung-Seob
간행물명
大韓韓醫學會誌
권/호정보
1999년|20권 1호|pp.44-51 (8 pages)
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정기간행물|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

Analysis of residual pesticides in herbal drugs was performed by GC-ECD and GC-MS. Especially, selected ion monitoring(SIM) technique was applied to increase the GC/MS sensitivity. Analysis of residual pesticides was determined sensitivity and selectively without any internal standard by setting the SIM technique to their characteristic fragments for quantitation ion and confirmation ion. The combination of two detector, GC-ECD and MS-SIM technique, is abailable for determining a multiclass residual pesticides in herbal drugs. The average recoveries through the method were $65.9%{sim}99.7%$ in herbal drugs. The data of gas chromatographic analysis was compared with the limits of residual pesticides in herbal drugs and agricultural foods. 4. 4-DDT was detected above the limits to the residual pesticides in herbal drugs. Diazinon and EPN were detected, but the limits of residual pesticides were less than that of agricultural foods.