- $WS_2$고체윤활제의 합성 및 구름베어링 적용
- ㆍ 저자명
- 신동우,윤대현,최인혁,김경도,정진수,정용선
- ㆍ 간행물명
- 윤활학회지
- ㆍ 권/호정보
- 1999년|15권 1호|pp.77-82 (6 pages)
- ㆍ 발행정보
- 한국윤활학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
The processing conditions fur the synthesis of platelet W $S_2$ lubricant powder through a solid-gas reaction were optimized. The mixture of tungsten and sulfur powders were sealed in a vacuum of 10$^{-6}$ torr, prior to heat-treating at 85$0^{circ}C$ fur 8 days. The reaction product showed a well-developed platelet W $S_2$ powder with an average size of 3.8 ${mu}{ extrm}{m}$. The TGA/DTA analysis of the synthesized W $S_2$ powder was performed up to 120$0^{circ}C$ at a rate of 1$0^{circ}C$/min in flowing air (100 ${mu}{ extrm}{m}$/min) atmosphere. The weight loss was about 6% up to 120$0^{circ}C$ compared to the original weight. A rapid weight loss of about 5% occurred in the temperature range of 44$0^{circ}C$ to 66$0^{circ}C$ and an exothermic peak observed due to the transition of W $S_2$ to W $O_3$. The synthesized W $S_2$powder was coated on the commercial deep grooved ball bearing (No. 6203) to examine the effect of W $S_2$, coating layer on the noise and endurance of the ball bearing. The level of noise obtained from W $S_2$, coated-ball bearing (56 ㏈) was higher. than the value (32 ㏈) occurred in the case of greece lubrication. The endurance of the ball-bearing assembled after the coating of W $S_2$ powder onto each part increased 50 times compared to the non-coated ball-bearing..