The purpose of this study is to investigate the thermal embrittlement and the mechanical properties of 2.25Cr-1Mo steel aged at high temperature for the extended periods. Original, aged artificiall y and used material were tested to obtain the tensile strength, hardness and impact absorbed energy. Tensile strength, hardness and impact absorbed energy decreased with the increasing aging time. The carbide morphology with the thermal embrittlement was found to contribute to the mechanical property change by X-Ray diffraction method.