- 탄화규소 나노섬유의 제조 및 물성
- ㆍ 저자명
- 신현익,송현종,김명수,임연수,이재춘
- ㆍ 간행물명
- 한국세라믹학회지
- ㆍ 권/호정보
- 2000년|37권 4호|pp.376-380 (5 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
Carbon nanofibers with an average diameter of 100nm were reacted with SiO vapor generated from a mixture of Si and SiO2 to produce silicon carbide nanofibers at temperature ranging 1200∼1500$^{circ}C$ under vacuum. The nanofiber reacted at 1200$^{circ}C$ for two hours consisted of silicon carbide with an average crystallite size of 10-20nm, amorphous silica and a significant amount of unreacted carbon. The surface area of silicon carbide nanofiber, obtained after removal of amorphous silica and unreacted carbon from converted carbon nanofibers at 1200$^{circ}C$, was as high as 150㎡/g. With increasing reaction temperature to 1500$^{circ}C$, the surface area was decreased to 14㎡/g. Growth of SiC crystallite size with increasing conversion temperature of carbon nanofiber was confirmed from Scherrer formula using the (111) diffraction line and TEM images of converted carbon nanofibers.