- 해조류중 흔적량 망간의 전열원자흡수 분광광도법 정량을 위한 매트릭스 개선에 관한 연구
- ㆍ 저자명
- 최종문,강동수
- ㆍ 간행물명
- 한국환경위생학회지
- ㆍ 권/호정보
- 2000년|26권 4호|pp.75-81 (7 pages)
- ㆍ 발행정보
- 한국환경보건학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
A matrix modification was studied for the determination of trace manganese in several seaweeds by electrothermal atomic absorption spectrophotometry(ETAAS). The type and quantity of modifiers were investigated to realize the efficient modification. Palladium was chosen as a single modifier. By the addition of palladium(5$mu extrm{g}$/$mell$) to 2ng/$mell$ manganese solution, the temperatures were raised from 1,00$0^{circ}C$ to 1,20$0^{circ}C$ for the charring and from 2,10$0^{circ}C$ to 2,20$0^{circ}C$ for the atomization as well as the sensitivity and reproducibility were improved. With such optimum conditions, the trace amount of manganese in several seaweeds(laver, tangle and brown seaweed) could be determined by a calibration curve method, and good recoveries of more than 965 were also obtained in the samples in which a given amount of manganese was spiked. The detection limit of this method was about 0.048ng/$mell$.