- 한약재중의 잔류농약 분석 - GC에 의한 18종 잔류농약의 분석 -
- ㆍ 저자명
- 황인숙,최병현,배청호,김명희,조해전,Hwang. In-Sook,Choi. Byung-Hyun,Bae. Chong-Ho,Kim. Myung-Hee,Cho. Hae-Jeon
- ㆍ 간행물명
- 생약학회지
- ㆍ 권/호정보
- 2001년|32권 3호|pp.200-211 (12 pages)
- ㆍ 발행정보
- 한국생약학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
This study was carried out to determine the 11 organochlorine, 7 organophosphorus residual pesticides in 251 crude drugs. These residual pesticides in herbal drugs were extracted with acetonitrile and the extracts were cleaned up via LC-florisil solid phase extraction column. The prepared samples were assayed for pesticide residues using GC-ECD, NPD with capillary column and identified by GC-MSD. Recoveries were $63.9{sim}111.5%$ in the organochlorine pesticides and $69.8{sim}92.4%$ in the organophosphorus pesticides, and detection limits were $0.001{sim}0.65;ppm$ in the organochlorine pesticides and $0.0009{sim}0.0074;ppm$ in the organophosphorus pesticides. Pesticide residues were detected in 9 cases.