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Preparation of Carbon Fiber from Heavy Oil Residue through Bromination
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  • Preparation of Carbon Fiber from Heavy Oil Residue through Bromination
  • Preparation of Carbon Fiber from Heavy Oil Residue through Bromination
저자명
Park. Young-Ok,Yang. Kap-Seung
간행물명
Fibers and polymers
권/호정보
2001년|2권 4호|pp.178-183 (6 pages)
발행정보
한국섬유공학회
파일정보
정기간행물|ENG|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

A pitch precursor for a general purpose carbon fiber was prepared by condensation of pyrolized fuel oil (petroleum residual oil) with bromine under nitrogen blowing. such a condensation raised the softening point of the pitch from 4$0^{circ}C$ to $265^{circ}$ with a yield of 43%. The pitch precurosr showed an enhanced aromaticity and enlarged molecular size, which led to a reduction in molecular mobility and optical isotropy. The precursor was spun into fibers of $20mu extrm{m}$ diameter at a take-up speed of 700m/min. The fiber was stepwise stabilized in air and carbonized in Ar gas to obtain an isotropic carbon fiber. The carbon fiber exhibited tensile strengths of 500-800 ㎫though the fiber was formed via a crude method. The electric conductivity of the carbon fiber was relatively high, 2.2$ imes$$10^2$S/cm, sufficient to be used as electrode materials.