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겔-케스팅한 알루미나 성형체에서 출발입도가 공정변수 및 성형 미세구조에 미치는 영향
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  • 겔-케스팅한 알루미나 성형체에서 출발입도가 공정변수 및 성형 미세구조에 미치는 영향
저자명
하창기,김재원,조창용,백운규,정연길,Ha. Chang-Gi,Kim. Jae-Won,Jo. Chang-Yong,Baek. Un-Gyu,Jeong. Yeon-Gil
간행물명
한국재료학회지
권/호정보
2001년|11권 10호|pp.869-878 (10 pages)
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한국재료학회
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

Alumina $(Al_2O_3)$ green bodies were fabricated by gel-casting using three kinds of alumina with different particle size (mean particle size: 4.6 $mu extrm{m}$, 0.32 $mu extrm{m}$, 10nm). The effects of particle size on gel-casting process and green microstructure were investigated. The optimum dispersion conditions using ammonium salt (D-3019) as dispersant were 0.2 wt% (4.63 $mu extrm{m}$), 0.5 wt% (0.32 $mu extrm{m}$), and 5.0 wt% (10 nm), in high solid loading. The optimum solid loading of each starting material for gel-casting was obtained as 59 vol% (4.63 $mu extrm{m}$), 57 vol% (0.32 $mu extrm{m}$), 15 vol% (10 nm), depending on particle size, indicating that nano-size particle (10 nm) represent lower solid loading as high specific surface area than those of other two starting materials. The drying at ambient conditions (humidity; $ hickapprox$90%) was performed more than 48hrs to enable ejection of the part from the mold and then at $120^{circ}C$ for 2hrs in an air oven, showing no crack and flaw in the dried green bodies. The pore size and distribution of the gelcast green bodies showed the significant decrease with decreasing particle size. Green microstructure was dependent on the pore size and distribution due to the particle size, and on the deairing step. The green density maximum obtained was 58.9% (4.63 $mu extrm{m}$), 60% (0.32 $mu extrm{m}$), 47% (10 nm) theoretical density (TD), and the deairing step applied before gel-casting did not affect green density.