- Oxalate 공침법에 의한 Gd2O3Doped CeO2의 미분말 합성 및 그 소결특성
- ㆍ 저자명
- 최광훈,박성용,이주진
- ㆍ 간행물명
- 전기전자재료학회논문지
- ㆍ 권/호정보
- 2002년|15권 1호|pp.46-55 (10 pages)
- ㆍ 발행정보
- 한국전기전자재료학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
10mo1% Gd$_2$O$_3$ doped CeO$_2$ fine powders were synthesized by the oxalate coprecipitation method. The characteristics and sintering behavior of fine powders were investigated. The oxalate precipitates had the specific surface area of 150$m^2$/g, and appeared to be fine and spherical primary particles with a size of approximately 5.5nm. The decomposition of the precipitates occurred from a temperature around 30$0^{circ}C$ and it was completed below 40$0^{circ}C$, resulted in the formation of the oxide. The calcination temperature of the fine powders was suitable at 77$0^{circ}C$. By introducing fine powders washed with alcohol and ball-milling process after calcination, the sintered body was possible to attain the value of 97% of the theoretical density at low temperature of 130$0^{circ}C$.