- 습식 환원법에 의한 니켈 미분말의 제조
- ㆍ 저자명
- 이윤복,문영태,신동우,김광호,Lee. Yoon-Bok,Moon. Young-Tae,Shin. Dong-Woo,Kim. Kwang-Ho
- ㆍ 간행물명
- 한국재료학회지
- ㆍ 권/호정보
- 2002년|12권 10호|pp.803-808 (6 pages)
- ㆍ 발행정보
- 한국재료학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
Nickel powders were prepared from nickel chloride solution by wet reduction process, and the size control of the particles was investigated with reactant concentration, dispersant agent, and the addition of ethanol as an organic solvent in NiCl$_2$ aqueous solution. The size of the particle decreased with the increase of nickel chloride concentration. Their average particle size were 1.9$mu extrm{m}$, 1.6$mu extrm{m}$ and $1.5mu extrm{m}$ with 0.5M, 0.8M and 1.0M of nickel chloride concentration respectively. The spherical particle was easily controlled by the addition of ethanol as an organic solvent. Especially, in 30 vol% of ethanol, the average particle size and specific surface area were about 0.2$mu extrm{m}$ and 8.98m$^2$/g, respectively.