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Effect of Si/α-Si3N4 Ratio on the Shape of Silicon Nitride Particles Produced by SHS Method
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  • Effect of Si/α-Si3N4 Ratio on the Shape of Silicon Nitride Particles Produced by SHS Method
  • Effect of Si/α-Si3N4 Ratio on the Shape of Silicon Nitride Particles Produced by SHS Method
저자명
Kim. Min-Sung,Park. Dong-Soo,Han. Byung-Dong,Kim. Hai-Doo,Park. Chan
간행물명
한국세라믹학회지
권/호정보
2002년|39권 3호|pp.217-221 (5 pages)
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한국세라믹학회
파일정보
정기간행물|ENG|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

Si and ${alpha}-Si_3N_4$ powder mixtures added with 3 wt% $Y_2O_3$ were reacted under 5 MPa nitrogen pressure. The reaction products contained ${alpha}-Si_3N_4$ particles with elongated shapes. Length and width of the elongated grains were the maximum when the starting powder mixture of 50 wt% Si - 47 wt% ${alpha}-Si_3N_4$ and 3 wt% $Y_2O_3$ was used. Aspect ratio of the elongated grains were between 4.4 and 5. When the starting powder mixture contained 70 wt% Si, large particles with irregular shapes appeared. Meanwhile, the reaction did not proceed when the starting powder mixture contained 30 wt% Si and less. The SHS product was easy to crush and the elongated particles obtained from the starting powder mixtures of 40 wt% Si - 57 wt% ${alpha}-Si_3N_4$ - 3 wt% $Y_2O_3$ and 50 wt% Si - 47 wt% ${alpha}-Si_3N_4$ - 3 wt% $Y_2O_3$ were good candidates for the seeds.