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Hydrothermal synthesis of $PbTiO_3$ oxides with perovskite structure
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  • Hydrothermal synthesis of $PbTiO_3$ oxides with perovskite structure
  • Hydrothermal synthesis of $PbTiO_3$ oxides with perovskite structure
저자명
Park. Sun-Min
간행물명
한국결정성장학회지
권/호정보
2003년|13권 1호|pp.24-30 (7 pages)
발행정보
한국결정성장학회
파일정보
정기간행물|ENG|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

The preparation of $PbTiO_3$ powder was carried out using the oxide starting material by hydrothermal method. The powder of a crystalline phase with perovskite structure was synthesized. The optimum conditions for the preparation of powder were as follows; hydrothermal solvent; 8M-KOH or 8M-NaOH, reaction temperature; 250~$270^{circ}C$, run time; 10 h. The ,shape of synthesized powders were well developed crystalline faces with specific surface area of about 2.3 $ extrm m^2$/g in KOH solution and about 5.0 $ extrm m^2$/g in NaOH solution. The cell parameters of powder were a = 3.90$AA$, c = 4.14 $AA$ and cell volume was 57.30 $AA^3$. The cell ratio (c/a) of powder was the same as the theoretical ratio with c/a = 1.06 and the phase transition temperature(Tc) of the powders was about $470^{circ}C$.