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DMMP 검출용 금속산화물을 첨가한 $SnO_2$ 가스센서 제조
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  • DMMP 검출용 금속산화물을 첨가한 $SnO_2$ 가스센서 제조
저자명
최낙진,반태현,곽준혁,백원우,김재창,허증수,이덕동
간행물명
韓國軍事科學技術學會誌
권/호정보
2003년|6권 3호|pp.54-61 (8 pages)
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한국군사과학기술학회
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

$SnO_2$ gas sensor for the detection DMMP, simulant of nerve gas was fabricated and its characteristics were examined. Sensing materials were $SnO_2$ added by TEX>$alpha$-$Al_{2}O_{3}$ with 0∼20wt.% and $In_{2}O_{3}$ with 0∼3wt.% and were physically mixed each material. They were deposited by screen printing method on alumina substrate. The sensor was consisted of sensing electrode with interdigit(IDT) type in front and a heater in back side. Its dimension was 7$ imes$10$ imes$0.6$ extrm{mm}^2$. Crystallite size 8t phase identification, specific surface area and morphology of fabricated $SnO_2$ powders were analyzed by X-ray diffraction(XRD), surface area analyzer(BET) and by a scanning electron microscope(SEM), respectively. Sensor was measured as flow type and sensor resistance change was monitored as real time using LabVIEW program. The best sensitivities were 75% at adding 4wt.% TEX>$</TEX>alpha$</TEX>-$Al_{2}O_{3}$, operating temperature $300^{circ}C$ and 87% at adding 2wt.% $In_{2}O_{3}$, operating temperature $350^{circ}C$ to DMMP 0.5ppm. Response and recovery times were about 1 and 3 min., respectively. Repetition measurement was very good with $pm$3% in full scale. As a result, operating temperature was lower TEX>$alpha$</TEX>-$Al_{2}O_{3}$ than $In_{2}O_{3}$, but sensitivity was higher $In_{2}O_{3}$ than $alpha$-$Al_{2}O_{3}$.