- DMMP 검출용 금속산화물을 첨가한 $SnO_2$ 가스센서 제조
- ㆍ 저자명
- 최낙진,반태현,곽준혁,백원우,김재창,허증수,이덕동
- ㆍ 간행물명
- 韓國軍事科學技術學會誌
- ㆍ 권/호정보
- 2003년|6권 3호|pp.54-61 (8 pages)
- ㆍ 발행정보
- 한국군사과학기술학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
$SnO_2$ gas sensor for the detection DMMP, simulant of nerve gas was fabricated and its characteristics were examined. Sensing materials were $SnO_2$ added by TEX>$alpha$-$Al_{2}O_{3}$ with 0∼20wt.% and $In_{2}O_{3}$ with 0∼3wt.% and were physically mixed each material. They were deposited by screen printing method on alumina substrate. The sensor was consisted of sensing electrode with interdigit(IDT) type in front and a heater in back side. Its dimension was 7$ imes$10$ imes$0.6$ extrm{mm}^2$. Crystallite size 8t phase identification, specific surface area and morphology of fabricated $SnO_2$ powders were analyzed by X-ray diffraction(XRD), surface area analyzer(BET) and by a scanning electron microscope(SEM), respectively. Sensor was measured as flow type and sensor resistance change was monitored as real time using LabVIEW program. The best sensitivities were 75% at adding 4wt.% TEX>$</TEX>alpha$</TEX>-$Al_{2}O_{3}$, operating temperature $300^{circ}C$ and 87% at adding 2wt.% $In_{2}O_{3}$, operating temperature $350^{circ}C$ to DMMP 0.5ppm. Response and recovery times were about 1 and 3 min., respectively. Repetition measurement was very good with $pm$3% in full scale. As a result, operating temperature was lower TEX>$alpha$</TEX>-$Al_{2}O_{3}$ than $In_{2}O_{3}$, but sensitivity was higher $In_{2}O_{3}$ than $alpha$-$Al_{2}O_{3}$.