The experimental investigation of a coal splitter used in the 500㎿(e) boilers of fossil power plant is carried out to validate the design criteria. To predict air flow and the amount of particles at the exit, velocity and the weight of particles are measured on test planes using the coal splitter model with two-dimensional phase doppler particle analyzer and the glass fiber filter. It is found that the position of guide plate influences significantly both flow rates of gas and particle at the exit. Gas flow rate was a linear function of the guide plate, whereas particle flow rate was a exponential function of it.