The devoicing vowel is a phonological process whose contrast in sonority is lost or reduces in a particular phonetic environment. Phonetically, the vocal fold vibration originates from the abduction/adduction of the glottis in relation to supraglottal articulatory movements. The purpose of this study is to investigate Korean vowel devoicing by means of experimental instruments. The interrelated laryngeal adjustments and aerodynamic effects for this voicing can clarify the redundant articulatory gestures relevant to the distinctive feature of sonority. Five test words were selected, being composed of the high vowel /i/, between the fricative and strong aspirated or lenis affricated consonants. The subjects uttered the test words successively at a normal or at a faster speed. The EMG, the sensing tube Gaeltec S7b and the High-Speech Analysis system and MSL II were used in these studies. Acoustically, three different types of speech waveforms and spectrograms were classified, based on the voicing variation. The intraoral air pressure curves showed differences, depending on the voicing variations. The activity patterns of the PCA and the CT for devoicing vowels appeared differently from those showing the partially devoicing vowels and the voicing vowels.