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$^2D$ NMR Probe Development for Investigation of Biosupramolecular Systems
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  • $^2D$ NMR Probe Development for Investigation of Biosupramolecular Systems
  • $^2D$ NMR Probe Development for Investigation of Biosupramolecular Systems
저자명
Kim. Andre,Kang. Shin-Won,Park. Jang-Su
간행물명
Journal of the Korean magnetic resonance society
권/호정보
2004년|8권 1호|pp.55-61 (7 pages)
발행정보
한국자기공명학회
파일정보
정기간행물|ENG|
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기타
이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

Biosupramolecular systems such as biological membranes usually fluid under physiological conditions$^1$. Therefore, solid-state NMR has been used to investigate biosupramolecular systems. But solid-state NMR spectra contain a large number of overlapping resonances and are rather difficult to analyze. These problem has to be overcome by selective isotope labeling. We constructed a deuterium NMR probe for AM400 NMR spectrometer, which is mainly used for liquid samples. To overcome the fluidity problem, a saddle type coil was designed. The efficiency was systematically investigated for two kinds of coil geometry, solenoid and saddle types. Our results suggest that solenoids are superior to saddle type coils in the sensitivity. However, the letter fits better to fluid samples such as biosupramolecular systems.