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액상환원법에 의한 CuO-H2O 슬러리로부터 미세 구리분말의 제조
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  • 액상환원법에 의한 CuO-H2O 슬러리로부터 미세 구리분말의 제조
저자명
안종관,김동진,이익규,이재령,양환진,Ahn. Jong-Gwan,Kim. Dong-Jin,Lee. Ik-Kyu,Lee. Jaeryeung,Huanzhen. Liang
간행물명
한국분말야금학회지
권/호정보
2005년|12권 3호|pp.192-200 (9 pages)
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한국분말야금학회
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

Ultrafine copper powder was prepared from $CuO-H_2O$ slurry with hydrazine, a reductant, under $70^{circ}C$. The influence of various reaction parameters such as temperature, reaction time, molar ratio of $N_2H_4$, PvP and NaOH to Cu in aqueous solution had been studied on the morphology and powder phase of Cu powders obtained. The production ratio of Cu from CuO was increased with the ratio of $N_2H_4/Cu$ and the temperature. When the ratio of $N_2H_4/Cu$ was higher than 2.5 and the temperature was higher than $60^{circ}C$, CuO was completely reduced into Cu within 40 min. The crystalline size of Cu obtained became fine as the temperature increase, whereas the aggregation degree of particles was increased with the reaction time. The morphology of Cu powder depended on that of the precursor of CuO and processing conditions. The average particle size was about $0.5;{mu}m$.