- Al-B-C 첨가 탄화규소의 스파크 플라즈마 소결에 의한 미세구조 발달
- ㆍ 저자명
- 조경식,이광순,이현권,이상진,최헌진,Cho. Kyeong-Sik,Lee. Kwang-Soon,Lee. Hyun-Kwuon,Lee. Sang-Jin,Choi. Heon-Jin
- ㆍ 간행물명
- 한국세라믹학회지
- ㆍ 권/호정보
- 2005년|42권 8호|pp.567-574 (8 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
Densification of SiC powder with additives of total amount of2, 4, 8 $wt\%$ Al-B-C was carried out by Spark Plasma Sintering (SPS). The unique features of the process are the possibilities of a very fast heating rate and a short holding time to obtain fully dense materials. The heating rate and applied pressure were kept at $100^{circ}C/min$ and 40 MPa, while the sintering temperature and holding time varied from 1700 - $1800^{circ}C$ for 10 - 40 min, respectively. The SPS-sintered specimens with different amount of Al-B-C at $1800^{circ}C$ reached near-theoretical density. The $3C{ ightarrow}6H,;15R{ ightarrow}4H$ phase transformation of SiC was enhanced by increasing the additive amount. The microstructure of SiC sintered up to $1750^{circ}C$ consisted of fine equiaxed grains. In contrast, the growth of large elongated grains in small matrix grains was shown in sintered bodies at $1800^{circ}C$, and the plate-like grains interlocking microstructure had been developed by increasing the holding time at $1800^{circ}C$. The grain growth rate decreases with increasing amount of Al-B-C in SiC starting powder, however, the both of volume fraction and aspect ratio of large grains in sintered body increased.