- 졸-겔법을 이용한 은 담지 하이드록시아파타이트의 제조
- ㆍ 저자명
- 문병배,김호건,Mun. Byung-Bae,Kim. Ho-Kun
- ㆍ 간행물명
- 한국분말야금학회지
- ㆍ 권/호정보
- 2005년|12권 6호|pp.428-432 (5 pages)
- ㆍ 발행정보
- 한국분말야금학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
In the present study, silver-doped antibacterial hydroxyapatites were successfully prepared by the sol-gel method. For the starting solution, the molar ratio of $Ca(NO_3)_2{cdot}4H_2O, P(OC_2H_5)_3,;C_2H_5OH,;and;H_O$ was set to 0.075:0.045:20:0.135; $AgNO_3$ was added to a ratio of Ag to total cation concentration of $0.5-12 mol\%$. The prepared sol was dried at $100^{circ}C$ for 48h and heat-treated at $1000^{circ}C$ for 2h to obtain particles in the 200-500nm size range. The product from the synthesis of silver-doped hydroxyapatite was investigated through X-ray diffraction experiments and scanning electron microscopy. The product showed high antibacterial properties, with a disinfection ratio of Staphylococcus aureus (ATCC 6538) and Escherichia coli (ATCC 25922) over $99.9^{circ}C$ as calculated from an antimicrobial effects evaluation by the shake flask method.