Mechanical properties of in-service facilities are required to evaluate the integrity of power plants and chemical plants. Non-destructive technique can be used to evaluate the mechanical properties. To investigate the mechanical properties using ultrasonic technique, the four classes of thermally aged specimens were prepared using an artificially accelerated aging method. Ultrasonic tests, tensile tests, fracture toughness tests, and hardness tests were performed for the specimens. Then the mechanical properties were compared with ultrasonic parameters such as attenuation and non-linear parameter. From the investigation, we confirm that the ultrasonic parameter can be used to evaluate the mechanical properties.