In this paper, we propose the calibration method of monopulse slope to minimize the variation of angle estimate in frequency agile noncoherent monopulse system. We analyze the monopulse slope characteristics of antenna and RF receiver including the phase and gain imbalances of each receiving channel and present the calibration method to minimize the phase and gain imbalances of RF receiver channels including antenna. In addition, we present the calibration method using channel switching to minimize the gain imbalance of IF receiver channels. The measured average monopulse slope within the frequency bandwidth is -0.96, the maximum variation of angle estimate is similar to theoretical value, $0.15^{circ}$ at ${pm}2^{circ}$ azimuth and $0.03^{circ}$ at $0^{circ}$ azimuth.