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Mo 나노분말의 소결거동 및 기계적 특성
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  • Mo 나노분말의 소결거동 및 기계적 특성
저자명
김해곤,김길수,오승탁,석명진,김영도,Kim. Hai-Gon,Kim. Gil-Su,Oh. Sung-Tag,Suk. Myung-Jin,Kim. Young-Do
간행물명
한국분말야금학회지
권/호정보
2007년|14권 6호|pp.386-390 (5 pages)
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한국분말야금학회
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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The sintering behavior and mechanical property of Mo nanopowder was investigated as a function of various sintering condition. Mo oxide nanopowders were milled using a high energy ball-milling process. After the ball milling for 20h, the crystalline size of $MoO_3$ was about 20 nm. The $MoO_3$ nanopowders were reduced at the temperature of $800^{circ}C$ without holding time in $H_2$ atmosphere. The sinterability of Mo nanopowder and commercial Mo powder was investigated by dilatometric analysis. Mo nanopowder and commercial Mo powder were sintered at $1200^{circ}C$ for 1 hand $1500^{circ}C$ for 3 h, respectively. In both specimens the measured relative density was about 95%. But the measured hardness values were 2.34 GPa for nanopowder and 1.87 GPa for commercial powder. Probably due to finer grain size of the sintered body prepared from Mo nanopowder than that prepared using commercial Mo powder. The mean grain sizes were measured to be about 1.4 mm and 6.2 mm, respectively.