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DCA-MOD 법으로 YBCO 박막 제조시 하소열처리의 승온속도 효과
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  • DCA-MOD 법으로 YBCO 박막 제조시 하소열처리의 승온속도 효과
  • Effect of heating rate on calcination heat treatment of YBCO thin films by DCA-MOD method
저자명
김병주,김혜진,조한우,권연경,유정희,이희균,홍계원,Kim. Byeong-Joo,Kim. Hye-Jin,Cho. Han-Woo,Kwon. Youn-Kyung,Ryu. Jung-Hee,Lee. Hee-Gyoun,Hong. Gye-Wo
간행물명
Progress in superconductivity
권/호정보
2007년|8권 2호|pp.186-192 (7 pages)
발행정보
한국초전도학회
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

High $J_c;YBa_2Cu_3O_{7-x}$ superconducting films have been fabricated $LaAlO_3(100)$ substrate by MOD method using dichloroacetic acid(DCA) as chelating solvent for preparing precursor solution. Heating rate was varied in order to optimize the calcination heat treatment condition in DCA-MOD method. Coated films were calcined at lower temperature up to $500^{circ}C$ in flowing humid oxygen atmosphere. The heating rate was calcined from $13.3^{circ}C/min;to;0.28^{circ}C/min$. Conversion heat treatment was performed $800^{circ}C$ for 2 h in flowing Ar gas containing 1000 ppm oxygen with a humidity of 9.45%. Surface and cross sectional SEM microstructures showed that particle sizes were increased with heating rate at a calcination step. The amount of pores was increased with heating rate in the calcined films. Dense microstructure and sharp texture were developed in an YBCO films after conversion heat treatment. A high critical current density (Jc) of $1.26MA/cm^2$ (@77 K and self-field) was obtained for the YBCO film which was prepared with a heating rate of $0.28^{circ}C/min$.