Experimental studies on the aerodynamic coupling effect on natural frequencies, critical speed and flutter instability of rotating disks are investigated in this paper. The theoretical analysis uses a fluid-structure model where the aerodynamic effects are represented in terms of elastic, lift and damping and stiffness components. The experiments performed using a vacuum chamber and ASMO/DVD disks rotating in vacuum, open and enclosure in several gaps with stationary wall give three main results. One is that the aerodynamic effect by the surrounding air reduces the natural frequencies and critical speeds of the vibration modes. The second is that natural frequency of disks rotating in open air is larger than that in enclosure. Finally, it is shown that the disk vibration is reduced as the gap between the disk and the rigid wall decreases.