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Synthesis of SnO2Microrods by the Thermal Evaporation of Sn Powders
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  • Synthesis of SnO2Microrods by the Thermal Evaporation of Sn Powders
  • Synthesis of SnO2Microrods by the Thermal Evaporation of Sn Powders
저자명
Kong. Myung-Ho,Kim. Hyoun-Woo
간행물명
한국재료학회지
권/호정보
2008년|18권 3호|pp.123-127 (5 pages)
발행정보
한국재료학회
파일정보
정기간행물|ENG|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

The production of tin oxide ($SnO_2$) microrods on iridium (Ir)-coated substrates was achieved through the thermal evaporation of Sn powders in which a sufficiently high $O_2$ partial pressure was employed. Scanning electron microscopy revealed that the product consisted of microrods with diameters that ranged from 0.9 to $40;{mu}m$. X-ray diffraction, high-resolution transmission electron microscopy, and selected area electron diffraction indicated that the microrods were $SnO_2$ with a rutile structure. As the microrod tips were free of metal particles, it was determined that the growth of $SnO_2$ microrods via the present route was dominated by a vapor-solid mechanism. The thickening of rod-like structures was related to the utilization of sufficiently high $O_2$ partial pressure during the synthesis process, whereas low $O_2$ partial pressure facilitated the production of thin rods.