- 초음파 분무열분해를 이용한 $MgB_2$ 분말 합성
- ㆍ 저자명
- 박성창,임영진,강성구,정준기,김찬중,김철진,Park. S.C.,Lim. Y.J.,Kang. S.G.,Chung. J.K.,Kim. C.J.,Kim. C.J.
- ㆍ 간행물명
- 한국초전도·저온공학회논문지
- ㆍ 권/호정보
- 2008년|10권 1호|pp.19-23 (5 pages)
- ㆍ 발행정보
- 한국초전도저온공학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
Spherical $MgB_2$ powders was synthesized with the ultrasonic spray pyrolysis(USP) process using aqueous solutions of boron and magnesium ion. The properties of synthesized $MgB_2$ powder were characterized by XRD, SEM and EDS. A small amount of MgO was detected as the secondary phase out of the synthesized powder and the ratios of $MgB_2$ to MgO increased with increasing furnace temperature. The particle size and morphology of $MgB_2$ powder were investigated with varying molar concentration of the boron and magnesium solution and furnace temperature between $600^{circ}C$ and $1000^{circ}C$ in $Ar/H_2$. The average particle size of $MgB_2$ showed narrow distribution ranging from 300nm to 400nm. The morphology of particles exhibited mostly spherical shapes and uniform distribution.