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Synthesis and Characterization of NixMn1-xFe2O4 Nanoparticles by a Reverse Micelle Process
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  • Synthesis and Characterization of NixMn1-xFe2O4 Nanoparticles by a Reverse Micelle Process
  • Synthesis and Characterization of NixMn1-xFe2O4 Nanoparticles by a Reverse Micelle Process
저자명
Kim. Sun-Woog,Kim. Hyeon-Cheol,Kim. Jun-Seop,Kim. Hyun-Ju,Bae. Dong-Sik
간행물명
한국재료학회지
권/호정보
2008년|18권 6호|pp.298-301 (4 pages)
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한국재료학회
파일정보
정기간행물|ENG|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

A preparation of $Ni_xMn_{1-x}Fe_2O_4$ nanoparticles produced via the reduction of Nickel nitrate hexahydrate, Manganese (II) nitrate hexahydrate and Iron nitrate nonahydrate with hydrazine in Igepal CO-520/cyclohexane reverse micelle solutions was investigated. Transmission Electron Microscope (TEM), X-ray Diffraction (XRD) and Vibration Sample Magnetometer (VSM) analyses showed that the resultant nanoparticles increased the molar ration of water to Igepal CO-520 as the concentrations of Nickel nitrate hexahyrate, Manganese (II) nitrate hexahydrate and Iron nitrate nonahydrate increased. The average size of the synthesized particles calcined at $600^{circ}C$ for 2hrs was in the range of 20 nm to 30 nm, and the particle distribution was broadened. The phase of the synthesized particles was crystalline, and the magnetic behavior of the synthesized particles was superparamagnetism. The effect of the synthesis parameters of the molar ratio of water to surfactant and the calcination temperature was discussed.