- 분말야금법으로 제조된 FeSi2 열전특성 화합물의 열처리 시간에 따른 미세조직과 상변화
- ㆍ 저자명
- 박경태,신진교,홍순직,천병선,Park. Kyoung-Tae,Shin. Jin-Gyo,Hong. Soon-Jik,Chun. Byong-Sun
- ㆍ 간행물명
- 한국분말야금학회지
- ㆍ 권/호정보
- 2010년|17권 6호|pp.482-488 (7 pages)
- ㆍ 발행정보
- 한국분말야금학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
In this study, $FeSi_2$ as high temperature performance capable thermoelectric materials was manufactured by powder metallurgy.The as-casted Fe-Si alloy was annealed for homogenization below $1200^{circ}C$ for 3 h. Due to its high brittleness, the cast alloy transformed to fine powders by ball-milling, followed by subsequent compaction (hydraulic pressure; 2 GPa) and sintering ($1200^{circ}C$, 12 h). In order to precipitate ${eta}-FeSi_2$, heat treatment was performed at $850^{circ}C$ with varying dwell time (7, 15 and 55 h). As a result of this experiment thermoelectric phase ${eta}-FeSi_2$ was quickly transformed by powder metallurgical process. There was not much change in powder factor between 7h and 55h specimens.